NMR Spectroscopy
About us
The Department of Chemistry of the University of Basel offers support in all aspects of NMR-spectroscopy to all its research groups. Every researcher has a personalized account on at least one instrument, in addition, group accounts exist on all open access spectrometers.
Advice and support in selecting, performing and interpreting NMR-experiments is provided and specialized pulse sequences are performed on demand.
We ask external groups or interested parties to contact us directly by email.
Methods
- one-, two-, three- and four-dimensional NMR experiments
- routine-2D-experiments (cosy, tocsy, noesy, roesy, hsqc, hmqc, hmbc)
- experiments with solvent suppression
- low and high temperature experiments (120 K – 400 K)
- diffusion ordered experiments (dosy)
- relaxation rates, kinetics and thermodynamic parameter determination
- 3D structure determination
- virtually all NMR-active nuclei (amongst others we perform: 1H, 2D, 3He, 6Li, 7Li, 10B, 11B, 13C, 14N, 15N, 17O, 19F, 21Ne, 23Na, 29Si, 31P, 37Cl, 51V, 55Mn, 57Fe, 59Co, 61Ni, 69Ga, 71Ga, 73Ge, 77Se, 103Rh, 107Ag, 109Ag, 113Cd, 115In, 119Sn, 129Xe, 183W, 187Os, 195Pt, 199Hg, 205Tl, 207Pb)
Scope of Analytes
- small organic molecules
- polymers
- inorganic metal complexes
- organometal compounds
- MOFs
- peptides
- proteins
- nucleic acids
- carbohydrates
- nano materials
User account
Please contact me via email to arrange a date for a safety briefing and the setup of your user account.
Contact
Prof. Dr. Daniel Häussinger
Tel.: +41 61 207 11 59
Email: daniel.haeussinger@clutterunibas.ch
Documents
Instruments
instrument | location | autosampler | open access | standard probe | additional probes |
---|---|---|---|---|---|
nmr 250MHz | OC 0a | BACS60 | yes | BBFO | QNP-DCN, BBI, BBO, LC-TXO, 3He-BBI, 10 mm low γ-BBO |
nmr 400MHz | OC 0b | BACS60 | yes | BBFO SP FB | QNP-CFP |
nmr 500MHz | OC 06 | BACS60 | yes | BBFO SP FB | BBl SP, BBI, BBO |
nmr 600MHz | OC 16 | - | no | BBFO SP | BBl, TXl, low γ-TBl-P, TBl-C |
nmr 400MHz | BPR-1060 | sample express | yes | BBFO SP FB | - |
nmr 500MHz | BPR-1096 | sample express | yes | BBFO SP FB | - |
nmr 600MHz | BPR-1096 | sample case | partially | QCl-F | 1.7 mm TCl |
All instruments are equipped with Bruker Avance III (HD) or Avance Neo consoles.